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Study Plan for Practical Work
This reaction should produce enough halogenoalkane to be able to use it in the next experiment.
Materials:
| 2-methylpropan-2-ol (20 cm3) | Concentrated hydrochloric acid (70 cm3) |
| Calcium chloride (6 g) | 0.1M sodium hydrogencarbonate (40 cm3) |
| Anhydrous sodium sulfate (5 g) | Anti-bumping granules |
| 100 cm3 measuring cylinder | 250 cm3 conical flask and bung |
| Funnel | 250 cm3 separating funnel |
| Bunsen burner | Mortar and pestle |
| Tripod and gauze | 100 cm3 conical flask |
| Heat proof mat | 25 cm3 & 100 cm3 measuring cylinders |
| Cotton wool | Glass bend |
| Still head | 50 cm3 pear-shaped flask |
| Liebig condenser | Rubber tubing |
| Sample bottle | 100 cm3 beaker |
| Joint clip | -10 to 110°C thermometer |
| Thermometer sleeve | Top pan balance reading to the nearest ± 0.1 g |